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Analytical center

Research areas

The main areas of activity of the Analytical Center (AC) of the FORC RAS are studies of the chemical composition and structure of materials at the macro-, micro-, and nano-levels, including:

  • Determination of chemical composition and impurity content by energy-dispersive X-ray microanalysis for various classes of materials, including nanomaterials
  • Characterization of the distribution of elements (from B to U) in different areas of the material
  • Phase determination, mapping of crystal orientations of grains, study of grain boundaries by electron backscatter diffraction
  • Obtaining microscopic images in electron beams in various modes, including in low vacuum mode, to characterize the surface properties of materials
  • Study of the phase composition and structure of samples by X-ray methods diffractometry
The objects of research are:
  • photonic crystal-based light guides and special fiber light guides;
  • new materials for fiber optics, quantum electronics, and other areas of modern science and technology;
  • nanomaterials and nanocrystalline inclusions in materials;
  • single crystals and composites;
  • cultural heritage objects
The Analytical Center conducts research on the topics of the General Physics Institute of the Russian Academy of Sciences and collaborates with a number of institutes of the Russian Academy of Sciences, universities, colleges, industrial enterprises, and firms. The Analytical Center is part of the Shared Use Center "Analytical Center of the General Physics Institute of the Russian Academy of Sciences." The AC services are presented on the CSEU website (https://www.gpi.ru/sci/cseu/)

Laboratory staff

Agakhanova Vitaliya A.

Research Fellow,
master

+7(499)503-87-45, доб. 3-09

vita@fo.gpi.ru
Head

Equipment

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Scanning electron microscope JSM-5910LV (JEOL) with analytical system Aztec ENERGY (OXFORD INSTRUMENTS) including EDS and WDS attachments for X-ray microanalysis and CRYSTAL attachment for electron backscatter diffraction studies.
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X-ray diffractometers
The D2 Phaser (Bruker AXS) allows a wide range of samples to be studied. The diffractometer is capable of performing various tasks: phase identification, microdiffraction analysis, texture and stress analysis, high-resolution X-ray diffractometry, indexing of X-ray patterns, Rietveld refinement and structure determination.
The D8 Discover is a multifunctional diffractometer offering micro X-ray diffraction analysis capabilities

Papers

  1. Iskhakova, L.D., Milovich, F.O., Likhachev, M.E., Lipatov D. S. Characteristics of the Composition and Structure of Core Glasses Activated with Rare-Earth Elements of Silicate Fiber //Glass Physics and Chemistry. 2022- Vol. 48 – Is. 5 - pp. 351-357. DOI:10.1134/S1087659622800033
  2. Plastinin E.A., Iskhakova L.D., Kashaykin P.F., Velmiskin, V.V., Firstov S.V., Milovich F.O. Ce-doped porous glass and optical fibers //Journal of Non-Crystalline Solids - 2022 - Vol. 579 - Paper121369 DOI:10.1016/j.jnoncrysol.2021.121369
  3. Plastinin, E.A., Velmiskin, V.V., Iskhakova, L.D., Kharakhordin, A.V., Semjonov, S.L. Bismuth-doped optical fiber from nanoporous glass with air cladding//Optical Engineering – 2022-Vol. 61 – Is. 3-paper 036108, DOI:10.1117/1.OE.61.3.036108
  4. Vakhrushev A.S., Umnikov A.A., Lobanov A.S., Firstova E.G., Evlampieva E.B., Riumkin K.E., Alyshev A.V., Khegai A.M., Guryanov A.N., Iskhakova L.D., Melkumov M.A., Firstov S.V. W-type and Graded-index bismuth-doped fibers for efficient lasers and amplifiers operating in E-band //Optics Express – 2022- Vol.30- Is. 2 - pp. 1490-1498. DOI:10.1364/OE.444360
  5. Vakhrushev A., UmnikovA., Alyshev S., Khegai A., Firstova E., Iskhakova L., Guryanov A., Melkumov M., Firstov, S. Double-Clad Bismuth-Doped Fiber with a Rectangular Inner Cladding for Laser Application // Photonics – 2022 – Vol. 9 – Is. 11- paper788 DOI:10.3390/photonics9110788
  6. Blagodarov S.V., Zheltukhina G.A., Romanova Y.M., Alekseeva,N.V., Iskhakova L.D., Semashko M.I., Tolordava E.R., Nebolsin V.E. Improving the synthesis of hemin derivatives and their effect on bacterial biofilms// Journal of Porphyrins and Phthalocyanines- 2022- Vol.26 – Is, 3, pp. 242-252. DOI:10.1142/S1088424622500079
  7. Il’in E.G., Parshakov A.S., Fatyushina E.V., Iskhakova L.D., Gryzlov D.Y., Milovich F.O. A New Method for the Synthesis of a NbC/C Nanocomposite //Inorganic Materials -2022- Vol. 58 – Is. 2 - pp. 190-198. DOI:10.1134/S0020168522020066
  8. Iskhakova L.D., Milovich F.O., Likhachev M.E., Lipatov D.S., Yashkov M.V., Lobanov A.S., Guryanov A.N. Analysis of elemental distributions and phase separation in rare-earth-doped silica-based fiber preforms and optical fibers. // Journal of Non-Crystalline Solids. – 2021. – Vol. 554. – Paper 120616. DOI:10.1016/j.jnoncrysol.2020.120616
  9. Shmorgun V.G., Bogdanov A.I., Kulevich V.P., Iskhakova L.D., Taube A.O. Microstructure and phase composition of diffusion coating formed in NiCr alloys by hot-dip aluminizing. // Surfaces and Interfaces. – 2021. – Vol. 23. – Paper 100988. DOI:10.1016/j.surfin.2021.100988
  10. Vagapova E.A., Strugovshchikov E., Orlovskaya E.O., Vanetsev A.S., Dolgov L., Puust L., Iskhakova L.D., Maeorg U., Pishtshev A., Orlovskii Y.V. Combined spectroscopic and DFT studies of local defect structures in beta-tricalcium phosphate doped with Nd(III). // Journal of Alloys and Compounds. – 2021. – Vol. 877. – Paper 160305. DOI:10.1016/j.jallcom.2021.160305.
  11. Voronina I.S., Dunaeva E.E., Papashvili A.G., Iskhakova L.D., Doroshenko M.E., Ivleva L.I. High-temperature diffusion doping as a method of fabrication of Ca-3(VO4)(2): Mn single crystals. // J. Cryst. Growth. – 2021. – Vol. 563. – Paper 126104. DOI:10.1016/j.jcrysgro.2021.126104
  12. Voronina I.S., Voronov V.V., Dunaeva E.E., Iskhakova L.D., Papashvili A.G., Doroshenko M.E, Ivleva L.I. Growth and properties of manganese doped Ca-3(VO4)(2) single crystals // J. Cryst. Growth. – 2021. – Vol. 555 – Paper 125965. DOI:10.1016/j.jcrysgro.2020.125965
  13. F.O. Milovich, L.D. Iskhakova, M.Y. Presniakov, A.L. Vasiliev, V.I. Bondarenko, S.E. Sverchkov, B.I. Galagan The identification of Bi atoms and clusters in Mg-Al silicate glasses //J. Non-Cryst. Solids -2019.- 510.- Р. 166-171 DOI:10.1016/j.jnoncrysol.2018.12.028
  14. L.D. Iskhakova, A.B. Ilyukhin, S.A. Kutovoi, V.I. Vlasov, Y.D. Zavartsev, V.F. Tarasov, R.M. Eremina The crystal structure of new quantum memory-storage material Sc1.368Y0.632SiO5 // Acta Crystallogr. C-Struct. Chem. 2019.- 75.- Р. 1202 DOI:10.1107/S2053229619010507
  15. L.D. Iskhakova, V.M. Mashinsky, F.O. Milovich, V.V. Velmiskin, E.A. Plastinin, S.V. Firstov, M.V. Lukashova, P.A. Somov, E.M. Dianov Microstructure, composition, and luminescent properties of bismuth-doped porous glass and optical fiber performs // J.. Non-Cryst. Solids 2019.-503.- Р. 28-35 DOI:10.1016/j.jnoncrysol.2018.09.022
  16. A.M. Balbashov, M.E. Voronchikhina, A.A. Mukhin, V.Y. Ivanov, L.D. Iskhakova Floating zone crystal growth and magnetic properties of M-type Co-substituted strontium hexaferrites» // J. Cryst. Growth. 2019.- 524.- UNSP 125158. DOI:10.1016/j.jcrysgro.2019.125158
  17. M.M. Khudyakov, A.S. Lobanov, D.S. Lipatov, A.N. Abramov, N.N. Vechkanov, A.N. Guryanov, M.A. Melkumov, K.K. Bobkov,S.S. Aleshkinal, T.A. Kochergina, L.D. Iskhakova, F.O. Milovich, M.M. Bubnov, M.E. Likhachev Single-mode large-mode-area Er-Yb fibers with core based on phosphorosilicate glass highly doped with fluorine //Laser Phys. Let. -2019.- 16.- 025105. DOI:10.1088/1612-202X/aaf7f8
  18. V. A.,MaslovV. V. Voronov, L. D. Iskhakova, E. G. Yarotskaya,P. P. Fedorov Mullite Synthesis from High-Temperature Solution // Inorganic materials 2019.-55. –P. 1151-1155 DOI:10.1134/S0020168519100091
  19. Дианов Е.М., Янг Л., Исхакова Л.Д., Вельмискин В.В., Пластинин Е.А., Милович Ф.О., Машинский В.М., Фирстов С.В. Использование нанопористых стекол для изготовления активных волоконных световодов, легированных висмутом с высокой концентрацией» // Квантовая электроника, 48(7), 658-661 (2018) DOI:10.1070/QEL16711
  20. Д. Ю. Ерин, О. Н. Егорова, Л. Д. Исхакова, Ф. О. Милович, С. Л. Семёнов, С. Г. Черноок, Активированные Yb3+ волоконные световоды с сердцевиной, изготовленной методом спекания порошков c вибрационным перемешиванием расплава // Оптический журнал 85(12) 69-75 (2018) DOI:10.17586/1023-5086-2018-85-12-69-76
  21. Исхакова Л.Д., Милович Ф.О., Ерин Д.Ю., Семёнов С.Л., Вельмискин В.В. Фазовое расслоение и кристаллизация фосфатно-силикатных стекол сердцевин преформ волоконных световодов // Физика и химия стекла, 44(2), 178-189 (2018).   DOI:10.1134/S1087659618020062
  22. Липатов Д.С., Абрамов А.Н., Гурьянов А.Н., Лобанов А.С., Бубнов М.М., Исхакова Л.Д., Лихачев М.Е., Исследование концентрационного предела вхождения Er2O3 и Yb2O3 в алюмофосфоросиликатное стекло Физика и химия стекла, т.44(6), стр. 26-34 (2018)
  23. L. D. Iskhakova,F. O. Milovich,D. Yu. Erin, V. V. Velmiskin, S. L. Semjenov, Phase Separation and Crystallization of Phosphate-Silicate Glass Cores of Preforms of Fiber Optics // Glass Phys.&Chem. 44(2), 137-144 (2018) DOI:10.1134/S1087659618020062
  24. L. D. Iskhakova, V. M. Mashinsky, F. O. Milovich, V. V. Velmiskin, E. A Plastinin, S. V. Firstov, M. V. Lukashova, P. A. Somov, E M. Dianov, Microstructure, composition, and luminescent properties of bismuth-doped porous glass and optical fiber performs // Journal of Non-Crystalline Solids, DOI:10.1016/j.jnoncrysol.2018.09.022
  25. Iskhakova L.D., Mashinsky V.M., Milovich F.O., Velmiskin V.V., Plastinin E.A., Firstov S.V., Lukashova M.V., Somov P.A., Dianov E.M., Microstructure, composition, and luminescent properties of bismuth-doped porous glass and optical fiber preforms // J Non-Crystalline Solids, (2018) DOI:10.1016/j.jnoncrysol.2018.09.022
  26. A. A. Mistonov,  A. P. Chumakov,R. P. Ermakov,L. D. Iskhakova, A. V.Zakharova, A. V. Chumakova, K. O.Kvashnina Electronic structure studies of bismuth compounds using high energy resolution X-ray spectroscopy and ab initio calculations // J. Alloys&Compounds, 753, 646-654 (2018) DOI:10.1016/j.jallcom.2018.04.190

Dissertations